Srinivasan nishi engineers pvt ltd india jan 4, 2010 email. Copper copper sulfate 16% sulfuric acid, astm a262 practice e strauss test this procedure is conducted to determine the susceptibility of austenitic stainless steel to inter granular attack associated with the precipitation of chromiumrich carbides. Astm a262 standard practices e test results, a condition 1, b condition 2, c condition 3, d condition 4. We report a specific time temperature heat treatments that result in brittle intergranular fracture of type 304 stainless steel by impact at liquid nitrogen temperature, by auger electron spectroscopy aes of four sensitized heats of the embrittled grain boundaries and icy the results of a corrosion test, %stm a262 practice e and c, on. A study on the failure of aisi 304 stainless steel tubes in a. The test may be conducted on any object to be tested that can be evacuated and to the other side of which helium or other tracer gas may be applied. The test employed a cylindrical aluminum aa2024t351 test specimen. In accordance with astm b117, astm b 368, astm g 85, din 50021, iso 10289, iso 9227, nen 10068 br, am 18 intergranular corrosion test strausstest sop 4010 in accordance with astm a262 practice e, iso 36512, din 50914 br, be, am, he, em 19 intergranular corrosion test streichertest sop 4011 in accordance with astm a262 practice b. Uns astm carbon manganese phosphorous sulfur silicon chromium nickel nitrogen s30100 301 0. Effect of carbon content on eddy current response to. A380a380m practice for cleaning, descaling, and passivation of stainless steel parts, equipment, and systems. The etch structure types used to classify the specimens are. The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular corrosion.
Astm g48 practicea and astm a262 practicec respectively, for the as cladded and liquid nitrided specimens. Al6xn alloy uns n08367 is a low carbon, high purity, nitrogenbearing superaustenitic stainless alloy. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric acid test for detecting susceptibility to intergranular attack was used. Nace mr 0175iso 15156 is a materials standard issued by the national association of corrosion engineers. As 15 hours is a difficult test period in practice, and is only a minimum. This paper investigates a failure in convection section tubes of a gas heater unit in a. Grain boundary chemistry is known to be a critical.
Duplex stainless steel welds and their susceptibility to. Astm a26215, standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, astm international, west conshohocken. Standard practices for detecting susceptibility to intergranular attack in. The huey test works astm a262 practice e to analyze chromium depleted regions and intermetallic astm a262 practice e, such as sigma phase, lractice is also used for materials in strongly oxidizing astm a262 practice e such as nitric acid. E3 guide for preparation of metallographic specimens.
As 15 hours is a difficult test period in practice, and is only a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent. Astm a262 astm b117 salt spray test astm b368 cass test astm g85 astm g85 a1 astm g85 a2 astm g85 a3 astm g85 a4 astm g85 a5 chemical testing corrosion testing metallography. A range of corrosion tests can be carried out inhouse including. Astm a262 method e is sometimes called the strauss test, and is the same as iso 36512 method a, except for the duration. Duplex stainless steels 97, maastricht, the netherlands, october. Is it acceptable for establish the pqr astm a 262 practice e for the material tp321 which contains titanium. Test intergranular corrosion o spindle mm length of period h 15 result of visual inspection at 20 x magnification after bend test absence of cracks heat treatment before test sensitization bend angle 0 produced without class 111 ozone depleting substances. Modified astm a262 standard practices ecoppercopper sulfate sulfuric acid test for detecting.
Standard test method for liquid penetrant examination se165 identical with astm speci. Resistant to inter granular corrosion astm a262 practice e. Where corrosion testing is required for sour service then the following can be subcontracted to other ukas accredited test facilities. Duplex stainless steel welds and their susceptibility to intergranular corrosion. Corrosion intergranular astm a262 corrosion stainless. Welding was performed using the manual gas tungsten arc welding. Practice ecoppercopper sulfatesulfuric acid test for detecting. Nace mr 0175iso 15156 for corrosion resistant alloys for. Astme498 standard practice for leaks using the mass. The microstructure evolution and its effect on corrosion properties of 18cr12ni2,5mo steel. The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular.
Igc test as per astm a 262 02a practice e showing 12 of 2 messages. The microstructure evolution and its effect on corrosion. Astm a262 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Test method b is used for testing vacuum systems either as a step in the final test of a new system or as a maintenance practice on equipment used for manufacturing, environmental test or for conditioning parts. A262 14 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, austenitic stainless steel, copper sulfate, corrosion testing, etch structures, ferric sulfate, intergranular corrosion, nitric acid, oxalic acid.
In accordance with astm a262 practice e, iso 36512, din 50914 br, be, am, he, em 19 intergranular corrosion test streichertest sop 4011 in accordance with astm a262 practice b, astm g28 br, be, am, he, em 20 intergranular corrosion test hueytest sop 4012 in accordance with astm a262 practice c, iso 36511 br, be. Astm a262 method c huey test is the same as that specified in iso 36511 not listed here. Astm a262 practice c stac spec 53961 astm a262 practice d astm a262 practice e. Two test methods namely a modified astm a262 and a modified double loop electrochemical potentiokinetic reactivation dlerp test were employed to determine the susceptibility to igc.
Choosing the correct method s rely on a complete understanding of your material and processes, as well as the. They observed that the reactivation method detects both continuous and local chromium depleted region in the steel structure, however acid test exposes only continuous depletion zones leading. Comparison of astm a262 practice a and analytical electron microscopy techniques b. The oxalic acid etch test is rapid and nondestructive, but not quantitative.
Duplex stainless steels 97, maastricht, the netherlands, october 1997. Streicher test astm a262 practice b generally used for stainless steel and nickel alloys, the streicher test involves boiling the specimen in a ferric sulfate sulfuric acid solution for 24120 hours and evaluating the results. Pdf duplex stainless steel welds and their susceptibility. Standard practice for liquid penetrant examination1. The astm a262 testing specification contains five unique intergranular corrosion tests. Comparison of astm a262 practice a and analytical electron microscopy techniques publication date. Automated image analysis software for assessing banding or orientation of microstructures in dual phase steel. The aged specimens were then subjected to astm a262 practice e test in a boiling 16 % h 2 so 4 solution containing 100 gl of cuso 4. The ballot has to pass the members of e28 and the members of the cos committee. Conducting the single loop slepr and double loop dlepr tests to detect the susceptibility of pitting and igc attack in stainless steel claddings as per astm g5 and astm g108 respectively, for the as cladded and nitrided. Pdf duplex stainless steel welds and their susceptibility to. For annual book of astm standards volume information, refer to the standards document summary page on the astm website. Report corrosion intergranular astm a262 please fill this form, we will try to respond as. Method a and astm a262 practice e 22 determination of the resistance to pitting corrosion ml 00223 astm g48 method a 23 determination of the freeiron content by ferroxyl test ml 34101 e astm a380 24 determination of the ferrite deltaferrite content ml 00302 e in house method astm e562 25 metal products metallographic researchml 00300 astm.
Magnified view of left convex surface and right crosssection of astm a262 practice e tested 304 stainless steel specimen in heat treated condition. Astm a262 intergranular corrosion testing and analysis. What is astm a262 intergranular corrosion test igc china. Discrepancies between the standard test astm a262 practice e and electrochemical reactivation test method was shown by novak et al. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric. Application and interpretation, astm manual series mnl 20, second edition. Astma262 standard practices for detecting susceptibility. Our stainless steel is capable of passing the intergranular corrosion test as per the astm a262 practice. The broad field of welding parameters for bohler cn 229 nfd permits universal application in a very wide range of wall. Astm a262 practice e strauss test this procedure is conducted to determine the susceptibility of austenitic stainless steel to inter granular attack associated with the precipitation of chromiumrich carbides. Standard practices for detecting susceptibility to.
Srinivasan nishi engineers pvt ltd india jan 4, 2010 e mail. Repeatability and reproducibility of compression strength. These specimens will have low corrosion rates in certain corrosion tests and therefore can be eliminated screened from testing as acceptable. Astm a262 practice a screening method has been used as advised by aydogdu and aydinol 2006 to know the susceptibility of the material towards intergranular corrosion.
Every batch of parker 6mo steel is tested for pitting corrosion as per the astm. A detailed study of aisi and stainless steels sss has been conducted to correlate the degree of sensitization dos measured by the. Pdf duplex stainless steels dss as alternatives to conventional austenitic. These practices include five intergranular corrosion tests, namely. Determination of susceptibility to intergranular corrosion. Astme498 your online library of us and international standards. Based on the appearance at the bend portion, the specimens were classified into four categories viz. It is originally a us standard intended to assess the suitability of materials for oilfield equipment where sulphide sulfide stress corrosion cracking may be. The al6xn alloy was designed to be a seawater resistant material and. Mar 19, 20 the aged specimens were then subjected to astm a262 practice e test in a boiling 16 % h 2 so 4 solution containing 100 gl of cuso 4. Characteristics and properties of stainless steel 3. Astm g48 practice a and astm a262 practice c respectively, for the as cladded and liquid nitrided specimens. Suppression of intergranular corrosion of 304 ss through laser.
This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is. Classification of the structure after a262 practice a analysis will determine if the material is acceptable or if additional testing is required. Standard practice for conditioning containers, packages. A370 test methods and definitions for mechanical testing of steel products.
For annual book of astm approved in last previous edition approved in as e 01. Astm news in actuality e 384 and e 92 are not to be married but e38410 will absorb e92 which dealt with macro vickers testing. Astm a 262 practice a was used for evaluation of the experimental steel to intergranular. However, epa would not accept the limited asbestos screen i. Active standard astm a262 developed by subcommittee. Tts diagram for aisi type 316 austenitic stainless steel established according to the test astm a262 practice a. Pdf corrosion intergranular astm a262 free download pdf. Uns astm carbon manganese phosphorous sulfur silicon chromium nickel nitrogen s30100. Oct 15, 2011 our client specification is silent about the igc test for the material astm a 312 tp321.
Th22600fv2stunterteihths527h fa tvorrichtung ths2602 ths260oc330af40 ths260fr5. Astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. Astme498 standard practice for leaks using the mass spectrometer leak detector or. Lowtemperature intergranular fracture and grain boundary. The microstructure evolution and its effect on corrosion properties of 18cr12ni2,5mo steel annealed at 500900c 126 in stainless steels refers to their susceptibility to intergranular corrosion resulting from microstructural changes. A study on the failure of aisi 304 stainless steel tubes in a gas. Astm a262 practice c 21 determination of the resistance to intergranular corrosion strauss test ml 00221 dinen iso 36512, method a and astm a262 practice e 22 determination of the resistance to pitting corrosion ml 00223 astm g48 method a 23 determination of the freeiron content by ferroxyl test ml 34101 e astm a380. E 01 standard practice for assessing the degree of bandin.
Astm a262 is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. An astm designation number identifies a unique version of an astm standard. Welding duplex stainless steel industry guide lasgroep regio. Tp 904 l a sa 269 a262 practice e s 31254 a sa 2 s 31803 a sa 789 p. Description download corrosion intergranular astm a262 comments. Corrosion intergranular astm a262 free download as pdf file. The al6xn alloy was designed to be a seawater resistant material and has since been demonstrated. This standard covers the practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
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